electrogravimetry

An Inexpensive Electrodeposition Device and Its Use in a Quantitative Analysis Laboratory Exercise

This experiment describes the construction of a simple apparatus for effecting the electrodeposition of nickel onto a tared copper electrode. Results are compared to the determination of nickel by the classical gravimetric precipitation of the dimethylglyoxime complex.

The full citation is here: Parker, R. H.  J. Chem. Educ. 2011, 88, 1428–1430 and a link to the article is provided below (subscription to the journal required).

http://dx.doi.org/10.1021/ed101202t